Authors :
Vishant Varma
Volume/Issue :
Volume 11 - 2026, Issue 3 - March
Google Scholar :
https://tinyurl.com/3y7mskcx
Scribd :
https://tinyurl.com/4esjd2fx
DOI :
https://doi.org/10.38124/ijisrt/26mar773
Note : A published paper may take 4-5 working days from the publication date to appear in PlumX Metrics, Semantic Scholar, and ResearchGate.
Abstract :
Growing environmental concerns have driven the development of sustainable nanoparticle synthesis methods,
with microwave-assisted green synthesis emerging as an efficient and eco-friendly approach. This technique combine rapid,
uniform microwave heating with green chemistry principles, decreases need of excess energy, waste production, and the use
of high-risk chemicals. In this study, Tinospora cordifolia stem extract used as a reducing and stabilizing agent, while ferric
(III) chloride (FeCl₃) used as the precursor reagent for the synthesis of iron oxide nanoparticles. Bioactive phytochemicals
such as phenolics and flavonoids facilitated the reduction of Fe³⁺ ions and prevented particle agglomeration. UV–Visible
spectroscopy (200–800 nm) confirmed nanoparticle formation, showing a characteristic absorption peak at 341.6 nm. SEM
(Scanning electron microscopy) explained the particles within the broad size range of 30–65 nm and variable surface
morphology. Overall, microwave irradiation enhanced reaction kinetics and enabled rapid, controlled, and sustainable
production of iron oxide nanoparticles.
Keywords :
Nanoparticles, Microwave, Green Chemistry, Environmental Remediation, phytochemical, therapeutic
References :
- Saod W. M., Al-Janaby M. S., Gayadh E. W., Ramizy A. and Hamid L. L. (2024) Biogenic synthesis of iron oxide nanoparticles using Hibiscus sabdariffa extract: Potential for antibiotic development and antibacterial activity against multidrug-resistant bacteria. Current Research in Green and Sustainable Chemistry 8 100397.
- Aigbe U. O. and Osibote O. A. (2024) Green synthesis of metal oxide nanoparticles, and their various applications. Journal of Hazardous Materials Advances 13 100401.
- Yilleng, Tm, Samuel, Ny, Stephen, D, Akande, Ja, Agendeh, Zm and Madaki, La, (2020) Biosynthesis of Copper and Iron Nanoparticles using Neem (Azadirachta indica) Leaf Extract and their Anti-bacterial Activity. J. Appl. Sci. Environ. Manage. 24 (11) 1987.
- Yassin M.T., Al-Otibi F.O. and Al–Askar A. A. (2024) Green synthesis, characterization and antimicrobial activity of iron oxide nanoparticles with tigecycline against multidrug resistant bacterial strains. Journal of King Saud University - Science 36 103131.
- Al-Karagoly H., Rhyaf A., Naji H., Albukhaty S., AlMalki F. A., Alyamani A. A., Albaqami J. and Alouf S. (2022) Green synthesis, characterization, cytotoxicity, and antimicrobial activity of iron oxide nanoparticles using Nigella sativa seed extract. Green Processing and Synthesis 11 254.
- Ikhuoria E. U., Uwidia I. E., Okojie R. O., Ifijen I. H., Chikaodili I. D. and Fatiqin A. (2024) Advancing Green Nanotechnology: Harnessing the Bio-reducing Properties of Musa paradisiaca Peel Extract for Sustainable Synthesis of Iron Oxide Nanoparticles. J. Multidiscip. Appl. Nat. Sci. 4(1) 108.
- Alijani H. Q., Pourseyedi S., Mahani M. T., Seifalian A. and Khatami M. (2020) Bimetallic nickel-ferrite nanorod particles: greener synthesis using rosemary and its biomedical efficiency, Artificial Cells. Nanomedicine, And Biotechnology 48(1) 242.
- Kamath V., Chandra P. and Jeppu G. P. (2020) Comparative study of using five different leaf extracts in the green synthesis of iron oxide nanoparticles for removal of arsenic from water. International Journal of Phytoremediation 22 1278.
- Yuvakkumar R. and Hong S. I. (2014) Green Synthesis of Spinel Magnetite Iron Oxide Nanoparticles. Advanced Materials Research 1051 39.
- Das M. P. and Rebecca L. J. (2018) Removal of Lead (II) by Phyto-inspired Iron Oxide Nanoparticles. Nature Environment and Pollution Technology 17 569.
- Bhuiyan M. S. H., Miah M. Y., Paul S. C., Aka T. D., Saha O., Rahaman M. M., Sharif M. J. I., Habiba O. and Ashaduzzaman M. (2020) Green synthesis of iron oxide nanoparticle using Carica papaya leaf extract: application for photocatalytic degradation of remazol yellow RR dye and antibacterial activity. Heliyon 6 e04603.
- Alexeree S. M. I., Abou‑Seri H. M., s EL‑Din H. E. M., Youssef D. and Ramadan M. A. (2024) Green synthesis of silver and iron oxide nanoparticles mediated photothermal efects on Blastocystis hominis. Lasers in Medical Science 39 42.
- Kuang Y, Wang Q, Chen Z, Megharaj M, Naidu R. (2013) Heterogeneous Fenton-like oxidation of monochlorobenzene using the green synthesis of iron nanoparticles. J Colloid Interface Sci. 410 67.
- Afsheen, S., Tahir M.B., Iqbal T.l, Liaqat A., Abrar M. (2018) Green synthesis and characterization of novel iron particles by using different extracts. J. Alloys Compd. 732 935.
- Karpagavinayagam P., Vedhi C., (2019) Green synthesis of iron oxide nanoparticles using Avicennia marina flower extract. Vacuum 160 286.
Growing environmental concerns have driven the development of sustainable nanoparticle synthesis methods,
with microwave-assisted green synthesis emerging as an efficient and eco-friendly approach. This technique combine rapid,
uniform microwave heating with green chemistry principles, decreases need of excess energy, waste production, and the use
of high-risk chemicals. In this study, Tinospora cordifolia stem extract used as a reducing and stabilizing agent, while ferric
(III) chloride (FeCl₃) used as the precursor reagent for the synthesis of iron oxide nanoparticles. Bioactive phytochemicals
such as phenolics and flavonoids facilitated the reduction of Fe³⁺ ions and prevented particle agglomeration. UV–Visible
spectroscopy (200–800 nm) confirmed nanoparticle formation, showing a characteristic absorption peak at 341.6 nm. SEM
(Scanning electron microscopy) explained the particles within the broad size range of 30–65 nm and variable surface
morphology. Overall, microwave irradiation enhanced reaction kinetics and enabled rapid, controlled, and sustainable
production of iron oxide nanoparticles.
Keywords :
Nanoparticles, Microwave, Green Chemistry, Environmental Remediation, phytochemical, therapeutic