Authors :
Sinan Sefertaş; Mehmet Yusuf Baran
Volume/Issue :
Volume 11 - 2026, Issue 7 - July
Google Scholar :
https://tinyurl.com/3tvt27wr
Scribd :
https://tinyurl.com/ynemwwc5
DOI :
https://doi.org/10.38124/ijisrt/26jul967
Note : A published paper may take 4-5
working days from the publication date to appear in PlumX Metrics, Semantic Scholar, and
ResearchGate.
Abstract :
This study investigates the gas nitriding process applied to C35 medium-carbon steel to improve the surface
properties of piston rods used in automotive tailgate and hood gas springs. In gas spring systems, the surface characteristics
of the piston rod, including hardness, wear resistance, low-friction behaviour, and corrosion resistance, have a direct
influence on system performance. In particular, micro-wear occurring at the rod–seal interface may lead to stick-slip
behavior, seal degradation, and reduced service life. In this study, C35 steel specimens were subjected to ferritic
nitrocarburizing followed by post-oxidation (FNC + ONC) at a constant treatment temperature with different ammonia
diffusion times. The nitriding treatments were performed at 570 °C for 2.45, 4.30, and 6.30 h. After treatment, the specimens
were characterized by Vickers microhardness measurements, optical microscopy, and neutral salt spray corrosion tests.
Surface hardness and compound (white) layer thickness were comparatively evaluated. The experimental results revealed
that the optimum ammonia diffusion time under the investigated processing conditions was 4.30 h at 570 °C, resulting in an
average surface hardness of 576 HV, a compound layer thickness of 18.3 μm, and a corrosion resistance of 168 h according
to ISO 9227. Furthermore, increasing the ammonia diffusion time led to higher surface hardness and a thicker compound
layer. These findings demonstrate that appropriate control of the ammonia diffusion time significantly enhances the surface
performance of gas-nitrided C35 steel while maintaining a compound layer suitable for gas spring applications.
Keywords :
Gas Nitriding; C35 Steel; Gas Spring; Ferritic Nitrocarburizing; Surface Hardness; Compound Layer;
References :
- D'Oliveira, A. S. C. M., Tschiptschin, C. P., & Bell, T. (2001). Gas nitriding of unalloyed and low alloy steels. Surface Engineering, 17(2), 147–152. https://doi.org/10.1179/026708401101517863
- Pye, D. (2003). Practical nitriding and ferritic nitrocarburizing. ASM International. https://doi.org/10.31399/asm.tb.pnfn.978162708350
- Fuhong Steel. (2026). C35 carbon steel (CK35 / DIN 1.0501): Properties and applications. https://www.round-bars.com/products/c35-carbon-steel-ck35-din-1-0501
- Mittemeijer, E. J., & Somers, M. A. J. (Eds.). (2014). Thermochemical surface engineering of steels: Improving materials performance. Woodhead Publishing.
- Child, H. C. (1980). Surface hardening of steel (Engineering Design Guides No. 37). Oxford University Press
- Davis, J. R. (Ed.). (2001). Surface engineering for corrosion and wear resistance. ASM International.
- Liedtke, D. (1995). Case hardening of steels: Bolt-on metallurgy. ASM International.
- Sun, Y., & Bell, T. (1991). Plasma surface engineering of low alloy steel. Materials Science and Engineering: A, 140, 419–434. https://doi.org/10.1016/0921-5093(91)90458
- Sirin, S. Y., Yildiz, K. C., & Alsaran, A. (2008). The effect of surface hardness and case depth on the fatigue performance of nitrided steels. Journal of Materials Science, 43, 2575–2580.
- Somers, M. A. J., & Mittemeijer, E. J. (1995). Layer-growth kinetics on gaseous nitriding of pure iron: Evaluation of diffusion coefficients for nitrogen in iron nitrides. Metallurgical and Materials Transactions A, 26(1), 57–74. https://doi.org/10.1007/BF02669794
- Alsaran, A., Karakan, M., & Çelik, A. (2002). The investigation of mechanical properties of ion-nitrided AISI 5140 low-alloy steel. Materials Characterization, 48(4), 323–327. https://doi.org/10.1016/S1044-5803(02)00275-9
- Skonieski, A. F. O., dos Santos, G. R., Hirsch, T. K., & da Rocha, A. S. (2013). Influence of gas nitriding parameters on the microstructure and hardness of carbon steels. Materials Research, 16(6), 1332–1339. https://doi.org/10.1590/S1516-14392013005000131
- Hossain, S., et al. (2006). Improving the corrosion resistance of carbon steel by gas nitriding. Surface and Coatings Technology, 201(6), 2824–2830.
- Deutsches Institut für Normung. (2006). DIN EN 10083-2:2006: Steels for quenching and tempering—Part 2: Technical delivery conditions for non-alloy steels.
- ASM International. (1991). ASM handbook (Vol. 4, Heat Treating, 10th ed.). ASM International.
- International Organization for Standardization. (2017). ISO 9227:2017. Corrosion tests in artificial atmospheres—Salt spray tests. International Organization for Standardization.
This study investigates the gas nitriding process applied to C35 medium-carbon steel to improve the surface
properties of piston rods used in automotive tailgate and hood gas springs. In gas spring systems, the surface characteristics
of the piston rod, including hardness, wear resistance, low-friction behaviour, and corrosion resistance, have a direct
influence on system performance. In particular, micro-wear occurring at the rod–seal interface may lead to stick-slip
behavior, seal degradation, and reduced service life. In this study, C35 steel specimens were subjected to ferritic
nitrocarburizing followed by post-oxidation (FNC + ONC) at a constant treatment temperature with different ammonia
diffusion times. The nitriding treatments were performed at 570 °C for 2.45, 4.30, and 6.30 h. After treatment, the specimens
were characterized by Vickers microhardness measurements, optical microscopy, and neutral salt spray corrosion tests.
Surface hardness and compound (white) layer thickness were comparatively evaluated. The experimental results revealed
that the optimum ammonia diffusion time under the investigated processing conditions was 4.30 h at 570 °C, resulting in an
average surface hardness of 576 HV, a compound layer thickness of 18.3 μm, and a corrosion resistance of 168 h according
to ISO 9227. Furthermore, increasing the ammonia diffusion time led to higher surface hardness and a thicker compound
layer. These findings demonstrate that appropriate control of the ammonia diffusion time significantly enhances the surface
performance of gas-nitrided C35 steel while maintaining a compound layer suitable for gas spring applications.
Keywords :
Gas Nitriding; C35 Steel; Gas Spring; Ferritic Nitrocarburizing; Surface Hardness; Compound Layer;